|
|
|
| |
|
|
CS-2000
Carbon
/ Sulfur Determinator |
Carbon/Sulfur
models
CS-530,
CS-2000
Carbon/Water
model
CW-800
Surface
Carbon model
SC-800
Oxygen/Nitrogen
models
ON-900,
ONH-2000
|
|
|
|
Overview |
|
The CS-2000 automatic analyser incorporates the latest
in combustion technology. It is designed for the rapid
simultaneous determination of carbon and sulfur in steel,
cast iron, copper, alloys, ores, cement, ceramics, carbides,
minerals, coal, coke, oil, ashes, catalysts, lime, gypsum,
soils, rubber, leaves, soot, tobacco, waste, sand, glass,
etc.
The CS-2000 can be supplied with up to four independent
infrared cells. The sensitivities of the cells resp.
the IR-absorbtion lengths can be individually selected
to offer optimum precision for the analysis of high
and low levels of both, sulfur and carbon. The CS-2000
features a microcontroller, a high temperature resistance
furnace up to 1550°C, an induction furnace and solid
state infrared detectors with auto zero and auto range
control. Separate cabinets eliminate any influence of
temperature between the resistance furnace and the analytical
unit. This modular design gives the user flexibility
to position the resistance furnace to the left or right
of the analyzer and also allows the installation of
a TIC-module between the two. The modular design makes
servicing much easier compared to single cabinet analyzers.
|
|
|
|
|
|
|
Operating technique |
Samples are accurately weighed in the ceramic crucible on
the interfaced electronic balance. By pressing a key, the
sample weight is automatically transfered to the PC. If required,
sample weights can also be entered manually. By pressing the
start key the analysis cycle begins and the sample enters
the furnace. Depending on sample weight and material analysed,
the typical analysis time is 50 seconds for induction furnace
operation and 60 to 120 seconds for resistance furnace operation.
During the analysis cycle instructions are displayed to ensure
easy and reliable performance. The CS-2000 requires minimal
maintenance for which access is simple. |
|
PC
control with Windows 2000/XP software |
Comprehensive
analyser control and easy operation are provided by
the software running on PC, connected to the analyser.
Click software
from the main menu for more information about software.
|
|
|
|
|
|
|
Infrared
Cells |
 |
|
The
infrared cells of the CS-2000 do not require any manual
zero adjustments. The zero and sensitivity adjustments
of the infrared cells are permanently and automatically
controlled by the electronics. The detectors utilize
solid state sensors combined with infrared filters.
The sensors are not gas filled, thus eliminating long
term problems due to gas leakage. The CS-2000 can be
equipped with up to four independent infrared cells.
The lengths of all four cells can be individually optimized,
to obtain maximum precision for the target analysis
levels of each customer. Each of the cells can be installed
with infrared absorption lengths ranging between 1mm
and 320mm. |
|
|
Resistance
Furnace up to 1550°C |
The
resistance furnace employs Silicon carbide heating elements.
Full electronic control includes current limitation during
cold-start conditions to promote long element life. A separate
sensor is used to monitor ambient temperature and provide
data for automatic reference point compensation ensuring that
furnace temperature is not affected by fluctuations of ambient
temperature. The furnace requires approximately 10 to 15 minutes
to reach operating temperature. |
|
Combustion
efficiency |
The
design of the resistance furnace boat stop ensures oxygen
carrier gas penetrates into the crucible, ensuring efficient
combustion. This design eliminates the need for fragile
lances and honeycomb boat stops which tend to block
easily with ash. Additionally the boat stop protects
the combustion tube from the aggressive combustion products,
thus extending the life of the tube. The combustion
tube is a simple straight ceramic tube that is robust
and inexpensive to replace. The life expectancy of the
tube is measured in thousands of analyses and not hundreds
as is the case with other analysers. (Protected by
German utility model)
|
|
 |
A
variety of combustion boats can be used in the furnace,
including the reusable ceramic boats (L=57 mm, W=22mm,
H=13 mm). Porcelain or quartz boats are also an
option. |
|
|
|
|
Automatic
induction furnace cleaning |
Users of carbon and sulfur analyzers with Induction
furnaces know that dust accumulates during combustion
and forms deposits (mainly of iron and tungsten oxides)
in the combustion chamber.
The CS-2000 furnace is cleaned automatically after each
analysis, thus ensuring repeatable and accurate results
without the time consuming and unpleasant task of manual
furnace cleaning.
The standard cleaning apparatus is mechanically attached
to the furnace open/close system, thus ensuring it is
not possible for the cleaning brush to collide with
a hot crucible.
|
|
|
The
cleaning brushes won't burn! |
The efficient design of the cleaning mechanism rules
out any possibility of the cleaning brush catching fire.
To confirm this fact, ELTRA offers free replacement
of each burned cleaning brush, during the entire working
life of the analyzer.
|
The
induction furnace and the autoloader use standard ceramic
crucibles, which are 1” or 25 mm in diameter. |
|
|
|
|
Fractional
analysis |
Due
to the fact that free carbon and sulfur burn at lower
temperatures than carbides and sulfates, the CS-2000
can separate and measure free carbon, free sulfur and
carbides and sulfates. After inserting the sample in
the combustion boat into the resistance furnace, the
boat gradually heats up. The free carbon and sulfur
within the sample burn first, while carbides and sulfides
burn several seconds later. The peak separation software
integrates the individual peaks and then displays the
results at the end of the combustion. |
|
|
|
|
Electronic
Flow Controller |
An
essential part of the gas flow system is the electronic flow
controller. This provides a stable gas flow by eliminating
the known disadvantages of mechanical controllers. |
|
Up
to 20 grams of copper sample without accelerators |
The
unique design of the induction furnace combined with intelligent
power control electronics enables the analysis of copper samples
up to a weight of 20 grams without the need of any accelerators.
This is very important in case of samples with extremely low
C and S contents, like copper and copper alloys. The higher
the weight, the higher the amount of C and S present. The
elimination of the need for an accelerator is a breakthrough
in the analysis of very low C and S. The use of accelerators
can badly affect the results when the very low C and S in
the sample is similar to the C and S content of the accelerators
(blanks). The CS-2000 eliminates this problem. |
|
Carrier
gas conservation |
If an analysis has not been carried our for a period oft time,
the analyzer will automatically switch to "gas conservation
mode.” This effectively means the carrier gas flow rate is
reduced to a minimum, only allowing a small amount of oxygen
to circulate through the IR cells etc. The period of time
before the gas conservation is activated, can be modified
via the PC software. It is also possible to have carrier gas
flow only during combustion. As soon as the next sample is
analyzed, the carrier gas returns to normal flow rate. |
|
TIC-module |
Due
to the modular design of the CS-2000, a module for total
inorganic carbon (TIC) can be placed between the resistance
furnace and the analyzer. For the TIC determination,
the sample is treated with acid in the TIC module. TIC
and total carbon (TC) can be alternately analyzed without
modifications. For TIC analysis the sample is treated
with acid in an Erlenmeyer flask inside the TIC-module.
The acid decomposes the carbonates in the sample, creating
CO2. The oxygen flow purges the CO2 out of the flask,
through to the infrared detector. TC is determined when
the sample is introduced into the furnace for combustion
and IR detection. |
|
 |
Analysis
procedure |
An
empty flask is placed on the balance. The tare button
is pressed. The sample is put into the flask. The sample
weight is entered into the analyzer by pressing a key.
A magnetic stirrer is placed into the flask. The flask
is attached to the TIC-module and the heated platform
is raised. The start key is pressed.
The acid is injected with the magnetic stirrer rotating.
The CO2 is released from the sample. The
infrared cell begins detection. When all the CO2
has been released from the sample, the detector`s signal
will return down to the baseline level and the analysis
will be terminated. |
|
|
Preheating crucibles |
 |
|
The
ceramic crucibles for the induction furnace can be preheated
in the high temperature furnace HTF-540. The preheating
reduces the blank value of the crucibles. This is important
for analysis in the very low ppm range. The crucibles
are inserted into the furnace tube and they remain preheated
in the tube until needed. Each time a crucible is needed,
a new one is inserted into the tube, and a preheated
crucible falls out the other end of the furnace tube.
The recommended preheating temperature is between 1250°C
and 1350°C. |
|
|
Auto
loader for the induction furnace |
|
|
The CS-2000 can be supplied with an automatic sample
loading system. This loading system may also be retrofitted
at a later date. The features of the loading system
are:
• Unlike many other auto loaders the ELTRA system can accomodate 130 samples giving hours of unattended operation. On request, the loader can be delivered for more crucibles.
• The auto loader, which does not occupy any additional bench space, is mounted above the area where the balance, PC, monitor and consumables are normally situated.
• The crucible positions in the loader are easily accesible to the operator even from a sitting position.
• Three available models for 130, 104 and 36 crucibles.
• Additional samples can be added whilst the system is running and the “out of the sequence” feature will allow urgent samples to be analysed immediately.
• Dispensers for accelerators are available. Depending on the applications, up to two dispensers can be attached to the analyser, for example, one for tungsten and one for iron accelerator. The dispensers are controlled by the loader software.
• Absolutely reliable.
• Reasonably priced.
For installing the auto loader, the resistance furnace should be positioned to the right of the analyser.
|
|
Compliance |
The CS-2000 complies to the specifications of the standards:
ISO-9556,
ISO-4935, ISO - 10694
ASTM
E-1019, E-1587, E-1915-97, D-1552, D-4239, D-5016, D-1619
DIN
EN 13137
UOP-703-98
PN-93
G-04514/17 |
| |
Next:
CS-2000 Specifications |
|  |
|